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Book 88001

Book 88001

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UNIVERSITY OF OKLAHOMA GRADUATE COLLEGE KINETIC DOPING OF SILICA SOL-GEL THIN FILMS AND APPLICATION AS BIOSENSORS A DISSERTATION SUBMITTED TO THE GRADUATE FACULTY In partial fulfillment of the requirements for the Degree of DOCTOR OF PHILOSOPHY By MATTHEW CROSLEY Norman, Oklahoma 2019 KINETIC DOPING OF SILICA SOL-GEL THIN FILMS AND APPLICATION AS BIOSENSORS A DISSERTATION APPROVED FOR THE DEPARTMENT OF CHEMISTRY AND BIOCHEMISTRY By Dr. Wai Tak Yip, Chair Dr. Ulrich H.E. Hansmann Dr. Charles V. Rice Dr. Robert L. White Dr. Lloyd A. Bumm © Copyright by MATTHEW CROSLEY 2019 All Rights Reserved TABLE OF CONTENTS Contents Chapter 1: SOL-GEL CHEMISTRY.............................................................................. 1 1.1 Sol-Gel Formation .............................................................................................. 1 1.2 Guest Molecules in a Sol-Gel Matrix ................................................................ 7 1.3 Sol-Gel Loading Methods .................................................................................. 9 1.4 Advantages to Sol-Gel Biosensors................................................................... 10 1.5 Kinetic Doping: Focus and Significance ........................................................ 13 1.6 References ......................................................................................................... 15 Chapter 2: TECHNIQUES AND INSTRUMENT SETUP .................... ...
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